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Background

Vat polymerization is one of the most popular 3D printing processes.  The lack of real-time tools to monitor the progress of stereolithography during printing and post-printing has been a challenge for increasing 3D printing reliability.  To overcome this challenge, LLNL researchers developed a monitoring method that uses a unique photo-physical phenomenon called Aggregation-Induced Emission (AIE), which enables fluorophores to increase its fluorescence upon aggregation in solution.

Description

Three important aspects of this invention are: (1) the formulation of a photocurable resin containing a fluorophore that exhibits AIE behavior; (2) the method of in-situ and real-time characterization for monitoring the reaction kinetics during the photopolymerization and UV-curing process; and (3) the application of a new 3D steganographic ink for 3D encrypted structure.

Image Caption: Shadowgraph Image from VAM (left).  Fluorescence Image from VAM (right). 

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Advantages

•    Value Proposition:  Real-time monitoring and characterization of photopolymerization processes.
•    Adaptable to material extrusion 3D printing
•    Since fluorescence can be detected only by fluorescence microscope, encrypted information would be undetected under standard optical microscopes.
 

Potential Applications

•    Vat polymerization 3D printers
•    Material Extrusion 3D printers
•    Two-Photon Lithography
•    Volumetric Additive Manufacturing
•    UV-coating
•    3D Information Encryption

Development Status

Current stage of technology development:  TRL 3 

LLNL has filed for patent protection on this invention.

Reference Number
IL-13880