LLNL researchers have developed a TDLAS-based, standalone, real-time gas analyzer in a small form-factor for continuous or single-point monitoring.  The system can analyze multiple gases with ultra-high sensitivity (ppm detection levels) in harsh conditions when utilizing wavelength-modulation spectroscopy (WMS). 

LLNL’s invention is a photopolymerizable polymer resin that consists of one or more nitrile-functional based polymers. The resin is formulated for SLA based 3D printing allowing for the production of nitrile-containing polymer components that can then be thermally processed into a conductive, highly graphitic materials. The novelty of the invention lies in (1) the photo-curable nitrile-…

LLNL researchers have developed a fabrication process for creating 3D random interdigitated architectures of anodes and cathodes, eliminating the need for a membrane to separate them.  This approach is similar to the repeating interdigitated multi-electrode architectures that also were developed at LLNL. 

LLNL researchers have developed novel advanced manufactured biomimetic 3D-TPMS (triply periodic minimal surface) membrane architectures such as a 3D gyroid membrane. The membrane is printed using LLNL's nano-porous photoresist technology.  LLNL’s 3D-TPMS membranes consist of two independent but interpenetrating macropore flow channel systems that are separated by a thin nano-porous wall.  3D-…

Improving the active material of the Zn anode is critical to improving the practicality of Zn-MnO2 battery technology. LLNL researchers have developed a new category of 3D structured Zn anode using a direct-ink writing (DIW) printing process to create innovative hierarchical architectures.  The DIW ink, which is a gel-based mixture composed of zinc metal powder and organic binders, is extruded…

This novel detector for characterizing IFE implosions is an alternative to the current RTNADs to measure neutron fluxes > 3x10¹¹ neutrons/cm² at high shot rates. The detector consists of a stack of small square metal wafers separated by thin insulating spacers. Every other wafer is held at high voltage while the remaining wafers are grounded. The stack acts as an…

To get the best of both worlds – the sensitivity of LC-MS with the speed of PS-MS – and a functional substrate that can maintain sample integrity, LLNL researchers looked to 3D printing.  They have patented a novel approach to create lattice spray substrates for direct ionization mass spectroscopy using 3D-printing processes.

LLNL researchers, through careful control over the chemistry, network formation, and crosslink density of the ink formulations as well as introduction of selected additives, have been successful in preparing 3D printable silicone inks with tunable material properties.  For DIW (direct in writing) applications, LLNL has a growing IP portfolio around 3D printable silicone feedstocks for diverse…

LLNL’s SAS technology embedded within a facility is developed to sense, detect, localize, alert, and communicate an active shooter(s) to first responders.  It relies on three integrated compact sensors that detect sound, infrared light (from the muzzle blast) and vibrations emanating from a gunshot.  Fusing the data from these detectors minimizes false alarms.

The key to time-reversal for an active shooter detection/tracking application is being able to estimate the space-time transfer function (Green’s function) between source-enclosure-receiver.  This approach begins with the acoustic mapping of an indoor muzzle blast. 

LLNL’s method of 3D printing fiber-reinforced composites has two enabling features:

LLNL researchers have designed and tested performance characteristics for a multichannel pyrometer that works in the NIR from 1200 to 2000 nm. A single datapoint without averaging can be acquired in 14 microseconds (sampling rate of 70,000/s). In conjunction with a diamond anvil cell, the system still works down to about 830K.

Scientists at Lawrence Livermore National Laboratory have developed a plastic that can detect neutrons, something previously thought impossible.

Livermore scientists demonstrated a plastic scintillator that can discriminate between neutrons and gamma rays with a polyvinyltoluene (PVT) polymer matrix loaded with a scintillating dye, 2,5-diphenyloxazole (PPO). They have found that…

The invention utilizes the statistical nature of radiation transport as well as modern processing techniques to implement a physics-based, sequential statistical processor. By this we mean that instead of accumulating a pulse-height spectrum as is done in many other systems, each photon is processed individually upon arrival and then discarded. As each photon arrives, a decision is…

LLNL's neutron "Pillar Detector" fabrication technology uses semiconductor-based micro-structured elements as an electrical signal generation medium for the detection of neutrons. These materials in the form of semiconductor "pillars" embedded in matrix of high cross-section neutron converter materials (such as Boron) that emit charged particles upon interaction with neutrons. These charged…

Transparent ceramic fabrication allows the production of gadolinium- , lutetium-, and terbium-based garnets which are difficult to grow by melt techniques due to phase instabilities. Phase stabilization of the garnets is accomplished by the addition of the intersubstitutional ions, Gallium and/or Scandium.

Scientists have developed many versatile and scaleable fabrication methods.…

LLNL's high fidelity hydrocode is capable of predicting blast loads and directly coupling those loads to structures to predict a mechanical response. By combining this code and our expertise in modeling blast-structure interaction and damage, along with our access to experimental data and testing facilities, we can contribute to the design of protective equipment that can better mitigate the…

LLNL researchers have grown and characterized scintillator crystals of Strontium Iodide (SrI2). Scintillator energy resolution and light yield proportionality surpass NaI and are similar to LaBr3. The SrI2 scintillators doped with europium (Eu) exhibit very high light yields (> 100,000 photons/MeV), extremely good energy resolution (<3% at 662 keV) and excellent light yield…

The LLNL detector measures radiation over a large dynamic range, spanning both high hazardous levels and weak levels, including natural background radiation. In weak radiation fields, the detector also measures gamma-ray spectra. The cost of the detector is significantly less than the total cost of existing separate detectors that could perform the same measurements.

LLNL's X-ray spectrometers based on STJ have been developed for high-resolution soft X-ray spectroscopy. STJ consist of two superconducting thin film electrodes separated by a thin insulating tunnel barrier. They measure X-ray energies from the increase in tunneling current after X-ray absorption in one of the electrodes excites additional charge carriers above the superconducting energy gap.…

LLNL has developed a radiation detector that cools to operating temperatures in 1-2 hours using two separate cooling stages. The first cooling brings the instrument to operating temperature. The embedded second cooling system achieves portable detection that can be sustained for 8-12 hours.

In addition, an integrated, hermetically-sealed package has been developed complete with…

LLNL has identified solution-grown organic crystals having scintillation efficiency not only close to, but even exceeding that of stilbene.. LLNL's invention relates to a new class of neutron detectors based on scintillation response of organic single crystals. More specifically, the use of organic molecules grown from solution and to molecules including the basic benzene or phenyl structure…

LLNL scientists have developed an approach for full spectrum analysis during gamma ray spectrometry using a spectral library signature created from a large amount of spectral data. The signature can be compared to unknown spectral measurements for the identification of previously unknown nuclear material.