Powder atomic layer deposition process is used to coat nanopowders of host materials (e.g. yttrium aluminum garnet) with optically active neodymium organometal precursor followed by O2/O3 RF plasma to convert to a single layer of Nd2O3. The process can be repeated to build arbitrarily thick layers with custom doping profiles and followed by post-…
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![Stock image UAV drone monitoring gas near pipeline valves](/sites/default/files/styles/scale_exact_400x400_/public/2024-04/UAV%20drone%20monitoring%20gas.jpg?itok=kdv1TGvJ)
LLNL researchers have developed a TDLAS-based, standalone, real-time gas analyzer in a small form-factor for continuous or single-point monitoring. The system can analyze multiple gases with ultra-high sensitivity (ppm detection levels) in harsh conditions when utilizing wavelength-modulation spectroscopy (WMS).
![Electrochemical CO2 conversion to valuable fuels and chemicals](/sites/default/files/styles/scale_exact_400x400_/public/2024-03/Electrochemical%20CO2%20conversion%20to%20valuable%20fuels%20and%20chemicals1.png?itok=G20rQOcY)
LLNL’s researchers use physical vapor deposition (sputter deposition or electron beam deposition) to coat an inert gasket material (i.e. PTFE) with a conductive metal (i.e. copper). The gas diffusion electrode overlaps onto the copper coated gasket to allow for electrical conductivity between the catalyst surface and the flow field/current collector of a CO2 electrolyzer. The coated gasket…
![SEM image of nanoporous Cu catalyst material](/sites/default/files/styles/scale_exact_400x400_/public/2024-02/SEM_nanoporous_Cu_catalyst.png?itok=xqwrkv1f)
Using their computational design optimization, LLNL researchers have developed copper-based dilute alloy catalysts (contains <10 at.% of the minority metal alloy component) and demonstrated these novel catalysts have improved energy efficiency and selectivity of the methane conversion reaction. By alloying copper with a small amount of the electropositive minority metal element, the…
![Laser peening induces deep compressive stress, which significantly extends the service lifetime over any conventional treatment](/sites/default/files/styles/scale_exact_400x400_/public/2024-02/laser%20peening%20inducing%20deep%20compressive%20stress.png?itok=oMzDBpkP)
This invention proposes using a pulse laser configured to generate laser pulses and a controller for controlling operation of the pulse laser. The controller is further configured to control the pulse laser to cause the pulse laser to generate at least one of the laser pulses with a spatiotemporally varying laser fluence over a duration of at least one of the laser pulses. The spatiotemporally…
![MonoTel Compact Monolithic Space Telescope](/sites/default/files/styles/scale_exact_400x400_/public/2024-01/MonoTel%20Compact%20Monolithic%20Space%20Telescope.png?itok=G-ETi6O8)
Rapid monolith development at scale is achieved through use of a functionally equivalent optic simulant made from a low-cost material to substitute the functional optic. Monolith optical performance is affected not only by thermal expansion but also by temperature inhomogeneity due to the temperature dependence of refractive index.
![MonoTel Compact Monolithic Space Telescope](/sites/default/files/styles/scale_exact_400x400_/public/2024-01/MonoTel%20Compact%20Monolithic%20Space%20Telescope.png?itok=G-ETi6O8)
Aeroptics are a proposed new class of monolithic optical system in aerogel fabricated by molding around a master mandrel. This approach combines the intrinsic stability of proven monolithic telescopes, with the ultralow density of silica aerogels. In Aeroptics, the monolith is hollow with an aerogel substrate providing a supporting structure. Theoretically, Aeroptics could enable 1-m aperture…
![MonoTel Compact Monolithic Space Telescope](/sites/default/files/styles/scale_exact_400x400_/public/2024-01/MonoTel%20Compact%20Monolithic%20Space%20Telescope.png?itok=G-ETi6O8)
This invention achieves both a wider field of view and faster f-number within a monolithic substrate by incorporating an aspheric convex refractive first surface and a planar aspheric field corrector surface on the final refractive surface. These two refractive surfaces work in conjunction with a concave aspheric primary and convex aspheric secondary mirror (e.g. Cassegrain type) to improve…
![Graphite](/sites/default/files/styles/scale_exact_400x400_/public/2023-09/graphite.jpg?itok=2CQBn1ca)
LLNL’s innovation offers an alternate synthetic route to graphite at lower cost using a molten salt mixture of CaCl2-CaCO3-CaO. The synthetic production of graphite and other high-value carbon materials is accomplished in molten salt media via electrochemical reduction and transformation of the carbon from the carbonate ion. The broad electrochemical window of molten salts enables the…
![National Ignition Facility (NIF)](/sites/default/files/styles/scale_exact_400x400_/public/2023-06/NIF.jpg?itok=Gem1TaQc)
This novel detector for characterizing IFE implosions is an alternative to the current RTNADs to measure neutron fluxes > 3x1011 neutrons/cm2 at high shot rates. The detector consists of a stack of small square metal wafers separated by thin insulating spacers. Every other wafer is held at high voltage while the remaining wafers are grounded. The stack acts as an…
![Projection Microstereolithographic Additively Manufactured Anion Exchange Membrane](/sites/default/files/styles/scale_exact_400x400_/public/2023-05/PuSL%20AEM.png?itok=kMLx_xAK)
The novel LLNL approach is to use projection microstereolithography (LAPµSL), starting with a photocurable methacrylate resin formulation consisting of a combination of a photoinitiator, photoabsorber, inhibitor, solvents, and other additives. Prior to use, the resin is pretreated to control viscosity for easier handling. The resin is fed to a LAPµSL printer which employs a near UV light…
![SEM image showing internal porosity of DIW printed parts](/sites/default/files/styles/scale_exact_400x400_/public/2023-05/internal%20porosity%20of%20DIW%20printed%20parts%20sq.png?itok=_QsLKjM7)
The inventors have developed a 3% Yttria partially-stabilized Zirconia (3YZ) ceramic ink that produces parts with both nano and microporosity and is compatible with two AM techniques: DIW and projection microstereolithography (PμSL). The 3YZ nano-porous ceramic printed parts had engineered macro cavities measuring several millimeters in length, wall thicknesses ranging from 200 to 540 μm, and…
![IPO logo over a face profile with interconnected lines](/sites/default/files/2020-11/IPO_logo_placeholder.jpg)
LLNL’s SAS technology embedded within a facility is developed to sense, detect, localize, alert, and communicate an active shooter(s) to first responders. It relies on three integrated compact sensors that detect sound, infrared light (from the muzzle blast) and vibrations emanating from a gunshot. Fusing the data from these detectors minimizes false alarms.
![IPO logo over a face profile with interconnected lines](/sites/default/files/2020-11/IPO_logo_placeholder.jpg)
The key to time-reversal for an active shooter detection/tracking application is being able to estimate the space-time transfer function (Green’s function) between source-enclosure-receiver. This approach begins with the acoustic mapping of an indoor muzzle blast.
![Microcapsules offer high surface area and a superior delivery system.](/sites/default/files/styles/scale_exact_400x400_/public/2020-11/Figure1IDEA.jpg?itok=9pdFUISw)
This invention describes a multiple nozzle microfluidic unit that allows simultaneous generation streams of multiple layered coaxial liquid jets. Liquids are pumped into the device at a combined flow rate from 100 mL/hr to 10 L/hr. Droplets are created with diameters in the range of 1 µm to 5 mm and can be created with 1-2 shell layers encapsulating fluid. Droplets created from the system can…
![creation of ultra-high energy density matter by an intense laser pulse](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/laser_update875.jpg?itok=793sEzmU)
![multichannel_pyrometer.jpg multichannel_pyrometer](/sites/default/files/styles/scale_exact_400x400_/public/2019-08/multichannel_pyrometer.jpg?itok=x0sCe_BN)
LLNL researchers have designed and tested performance characteristics for a multichannel pyrometer that works in the NIR from 1200 to 2000 nm. A single datapoint without averaging can be acquired in 14 microseconds (sampling rate of 70,000/s). In conjunction with a diamond anvil cell, the system still works down to about 830K.
![monolithic_telescope.png monolithic_telescope](/sites/default/files/styles/scale_exact_400x400_/public/2019-08/monolithic_telescope.png?itok=s7ZajArc)
Monolithic Telescopes are a novel implementation of a solid catadioptric design form, instantiated in a monolithic block of fused silica.
![nuclear reactor](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/nuclear%20reactor.jpg?itok=RMgGfrZv)
The new LLNL technique works by transiently removing and trapping concrete or rock surface material, so that contaminants are confined in a manner that is easy to isolate and remove. Our studies suggest that 10 m2 of surface could be processed per hour. The technique easily scales to more surface/hr.
![Next generation pillar detector](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/next-generation%20pillar%20detector.jpg?itok=7NBEyiYS)
LLNL's neutron "Pillar Detector" fabrication technology uses semiconductor-based micro-structured elements as an electrical signal generation medium for the detection of neutrons. These materials in the form of semiconductor "pillars" embedded in matrix of high cross-section neutron converter materials (such as Boron) that emit charged particles upon interaction with neutrons. These charged…
![Transparent Scintillators](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/Transparent%20Scintillators.jpg?itok=YDhoI0XA)
Transparent ceramic fabrication allows the production of gadolinium- , lutetium-, and terbium-based garnets which are difficult to grow by melt techniques due to phase instabilities. Phase stabilization of the garnets is accomplished by the addition of the intersubstitutional ions, Gallium and/or Scandium.
Scientists have developed many versatile and scaleable fabrication methods.…
![Marine helmet](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/Marine%20helmet-inside.jpg?itok=8W_dqpgI)
LLNL's high fidelity hydrocode is capable of predicting blast loads and directly coupling those loads to structures to predict a mechanical response. By combining this code and our expertise in modeling blast-structure interaction and damage, along with our access to experimental data and testing facilities, we can contribute to the design of protective equipment that can better mitigate the…
![Natalia Zaitseva examines a single crystal growing in a solution-growth crystallizer developed for production of stilbene crystals for fast neutron detection](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/solution-growth%20crystallizer.jpg?itok=SlXZs_1s)
LLNL researchers have grown and characterized scintillator crystals of Strontium Iodide (SrI2). Scintillator energy resolution and light yield proportionality surpass NaI and are similar to LaBr3. The SrI2 scintillators doped with europium (Eu) exhibit very high light yields (> 100,000 photons/MeV), extremely good energy resolution (<3% at 662 keV) and excellent light yield…
![Radiation Sign](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/Radiation%20Sign.jpg?itok=_mPjSajQ)
The LLNL detector measures radiation over a large dynamic range, spanning both high hazardous levels and weak levels, including natural background radiation. In weak radiation fields, the detector also measures gamma-ray spectra. The cost of the detector is significantly less than the total cost of existing separate detectors that could perform the same measurements.
![STJ x-ray spectrometer (shown on the table) to characterize a material sample.](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/STJ%20x-ray%20spectrometer.jpg?itok=OEllnuT5)
LLNL's X-ray spectrometers based on STJ have been developed for high-resolution soft X-ray spectroscopy. STJ consist of two superconducting thin film electrodes separated by a thin insulating tunnel barrier. They measure X-ray energies from the increase in tunneling current after X-ray absorption in one of the electrodes excites additional charge carriers above the superconducting energy gap.…
![gemini.jpg gemini](/sites/default/files/styles/scale_exact_400x400_/public/2019-08/gemini.jpg?itok=elYbWcjz)
LLNL has developed a radiation detector that cools to operating temperatures in 1-2 hours using two separate cooling stages. The first cooling brings the instrument to operating temperature. The embedded second cooling system achieves portable detection that can be sustained for 8-12 hours.
In addition, an integrated, hermetically-sealed package has been developed complete with…
![Natalia Zaitseva examines a single crystal growing in a solution-growth crystallizer developed for production of stilbene crystals for fast neutron detection](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/solution-growth%20crystallizer.jpg?itok=SlXZs_1s)
LLNL has identified solution-grown organic crystals having scintillation efficiency not only close to, but even exceeding that of stilbene.. LLNL's invention relates to a new class of neutron detectors based on scintillation response of organic single crystals. More specifically, the use of organic molecules grown from solution and to molecules including the basic benzene or phenyl structure…
![Truck approaching radiation portal monitor](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/Truck%20approaching%20radiation%20portal%20monitor.jpg?itok=gULQckpn)
LLNL scientists have developed an approach for full spectrum analysis during gamma ray spectrometry using a spectral library signature created from a large amount of spectral data. The signature can be compared to unknown spectral measurements for the identification of previously unknown nuclear material.
![Laser Peening](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/Laser%20peening.jpg?itok=l2OKtGme)
LLNL’s system consists of one or more flashlamp-pumped Nd:glass zig-zag amplifiers, a very low threshold stimulated-Brillouin-scattering (SBS) phase conjugator system, and a free-running single frequency Nd:YLF master oscillator.
![plastic_scintillators.jpg plastic_scintillators](/sites/default/files/styles/scale_exact_400x400_/public/2019-08/plastic_scintillators.jpg?itok=_aZx24vp)
Scientists at Lawrence Livermore National Laboratory have developed a plastic that can detect neutrons, something previously thought impossible.
Livermore scientists demonstrated a plastic scintillator that can discriminate between neutrons and gamma rays with a polyvinyltoluene (PVT) polymer matrix loaded with a scintillating dye, 2,5-diphenyloxazole (PPO). They have found that…
![Space-based Telescopes for Actionable Refinement of Ephemeris (STARE)](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/STARE.jpg?itok=nUdNYjfG)
LLNL is developing the Space-based Telescopes for Actionable Refinement of Ephemeris (STARE). STARE is a constellation of low cost nano-satellites (less than 5Kg) in low-earth orbit dedicated to the observation of space debris in conjunction with a ground-based infrastructure for maintenance, coordination and data processing. Each nano-satellite in the constellation is capable of recording an…
![Radio Active Materials processed](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/Radio%20Active%20Materials%20processed_0.jpg?itok=ESogQosQ)
The invention utilizes the statistical nature of radiation transport as well as modern processing techniques to implement a physics-based, sequential statistical processor. By this we mean that instead of accumulating a pulse-height spectrum as is done in many other systems, each photon is processed individually upon arrival and then discarded. As each photon arrives, a decision is…