Powder atomic layer deposition process is used to coat nanopowders of host materials (e.g. yttrium aluminum garnet) with optically active neodymium organometal precursor followed by O2/O3 RF plasma to convert to a single layer of Nd2O3. The process can be repeated to build arbitrarily thick layers with custom doping profiles and followed by post-…
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![Laser peening induces deep compressive stress, which significantly extends the service lifetime over any conventional treatment](/sites/default/files/styles/scale_exact_400x400_/public/2024-02/laser%20peening%20inducing%20deep%20compressive%20stress.png?itok=oMzDBpkP)
This invention proposes using a pulse laser configured to generate laser pulses and a controller for controlling operation of the pulse laser. The controller is further configured to control the pulse laser to cause the pulse laser to generate at least one of the laser pulses with a spatiotemporally varying laser fluence over a duration of at least one of the laser pulses. The spatiotemporally…
![Examples of different UV exposure patterns printed from the same multi-material resin. Darker yellow regions have higher UV exposure times leading to tougher regions.](/sites/default/files/styles/scale_exact_400x400_/public/2024-01/UV%20exposure%20patterns.jpg?itok=gxDjP8_E)
LLNL researchers have developed an innovative and uniform single-pot polymer multi-material system, based on a combination of 3 different reactive chemistries. By combining the three different constituent monomers, fine control of mechanical attributes, such as elastic modulus, can be achieved by adjusting the dosage of UV light throughout the additive manufacturing process. This results in…
![Top down view of a Gas phase synthesized graphene (GSG) UV curable polymer composite film.](/sites/default/files/styles/scale_exact_400x400_/public/2024-01/GSG%20UV%20curable%20polymer%20composite%20film.jpg?itok=9K-LMcLo)
LLNL researchers have developed a method to incorporate gas phase synthesized graphene (GSG) as a unique additive in a UV-crosslinkable polymer formulation. The GSG is added by using a planetary mixer to obtain a homogenous suspension of GSG in polymer. The resulting formulation is highly stable and doesn't show signs of phase separation or solid sedimentation. The polymer formulation is then…
![SEM image of tantalum airbridges](/sites/default/files/styles/scale_exact_400x400_/public/2023-12/SEM%20image%20of%20tantalum%20airbridges.png?itok=ZSZvL90K)
LLNL researchers developed a novel method to nucleate the alpha phase of Tantalum on a polymer surface at room temperature, allowing for the controllable formation of a variety of 3D structures, such as airbridges. Using this method with a subsequent Piranha etch results in the complete removal of the residues of the polymer 'scaffolding' or template while allowing the deposited tantalum…
![Powder in Chemical Watch Glass](/sites/default/files/styles/scale_exact_400x400_/public/2023-12/gray%20powder.jpeg?itok=u_5ZtG7H)
LLNL researchers have developed a Li-Sn-Zn ternary alloy and its method of production. Instead of traditional alloying techniques, the alloy was synthesized using mechanical alloying (high energy ball milling). With high purity elemental powders of lithium, tin and zinc, LLNL researchers were able to prepare Li60Sn20Zn20 as well as Li70Sn20Zn10 nanopowders.
![Scanning electron microscopy image of carbonized resorcinol-formaldehyde formulation.](/sites/default/files/styles/scale_exact_400x400_/public/2023-07/SEM%20image%20of%20carbonized%20resorcinol-formaldehyde%20formulation.png?itok=46D5k1qt)
LLNL inventors have created innovative steps in the synthesis, carbonation and activation steps of aerogel manufacturing that allows for large scale production. These steps are:
1. Synthesis: a novel pre-cure step with subsequent gelation (RF precursor solution is heated with stirring to achieve a mixed liquid intermediate temperature, the precursor solution is then allowed to cool,…
![Livermore researchers support efforts to limit the need for rare-earth elements in U.S. clean-energy technologies.](/sites/default/files/styles/scale_exact_400x400_/public/2023-07/Reducing%20Reliance%20on%20Critical%20Materials.png?itok=IuC6bH4r)
CMI—a DOE Energy Innovation Hub—is a public/private partnership led by the Ames Laboratory that brings together the best and brightest research minds from universities, national laboratories (including LLNL), and the private sector to find innovative technology solutions to make better use of materials critical to the success of clean energy technologies as well as develop resilient and secure…
![A sample of micro-architectured graphene aerogel, made from one of the lightest materials on Earth, sits atop a flower.](/sites/default/files/styles/scale_exact_400x400_/public/2023-06/micro-architectured%20graphene%20aerogel.jpg?itok=t56kL59Q)
To overcome challenges that existing techniques for creating 3DGs face, LLNL researchers have developed a method that uses a light-based 3D printing process to rapidly create 3DG lattices of essentially any desired structure with graphene strut microstructure having pore sizes on the order of 10 nm. This flexible technique enables printing 3D micro-architected graphene objects with complex,…
![Biosorption-based REE recovery and Sc extraction from low-grade feedstocks.](/sites/default/files/styles/scale_exact_400x400_/public/2023-06/Biosorption-based%20Sc%20separation.png?itok=nULPXLYl)
The novel technology developed at LLNL is a new, effective means of separating and concentrating Sc from lanthanides and non-REEs in unconventional, waste-derived feedstocks, thereby transforming an essentially valueless solution into valuable Sc concentrates. The results represent an important advance in the development of an environmentally sustainable alternative to organic solvent-based…
![natural protein lanmodulin, LanM (blue) bound to three REE ions (cyan).](/sites/default/files/styles/scale_exact_400x400_/public/2023-05/LanMwithREEions.png?itok=UcejC0kj)
LLNL researchers along with collaborators at Pennsylvania State University have found that a newly discovered natural protein named Lanmodulin (LanM) could be a potential candidate for extracting REEs from ore or other sources such as coal ash as well as purifying the REE material. Through joint research, the scientists found that LanM undergoes a large conformational change in response to…
![IPO logo over a face profile with interconnected lines](/sites/default/files/2020-11/IPO_logo_placeholder.jpg)
LLNL researchers have developed a custom formulated extreme low viscosity reactive silicone resin base modified with a temperature dependent thixotrope along with a modified catalyst package. The uncatalyzed composition is capable of accepting loadings of polymer microspheres sufficient to produce a cured bulk rubber that has a density as low as 0.3 g/cc, thus compatible with high-resolution…
![Flexible optoelectronic chip with integrated transmitter and receiver subassemblies](/sites/default/files/styles/scale_exact_400x400_/public/2023-04/Flexible_optoelectronic_chip.png?itok=EVf8ujMo)
Commercial fiber optic cables are the current standard for carrying optical signals in industries like communications or medical devices. However, the fibers are made of glass, which do not have favorable characteristics for applications that require flexibility and re-routing, e.g. typically brittle, limited selection of materials, dimension constraints.
![Mycobacterium tuberculosis](/sites/default/files/styles/scale_exact_400x400_/public/2022-07/Tuberculosis.jpg?itok=Am8SJWPD)
LLNL researchers have developed a high-volume, low-cost diagnostic test that is easy to use and provides results in under an hour. The testing platform will provide emergency responders and other medical professionals with the ability to screen individuals using oral and nasal samples, and obtain results in approximately 30 minutes. This point-of-care testing approach will enable rapid triage…
![creation of ultra-high energy density matter by an intense laser pulse](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/laser_update875.jpg?itok=793sEzmU)
![DNA](/sites/default/files/styles/scale_exact_400x400_/public/2022-07/DNA.jpg?itok=ES9MRz5G)
LNLL scientists have invented a method for multiplexed detection of PCR amplified products which can be completed in a single step. Highly validated species-specific primer sets are used to simultaneously amplify multiple diagnostic regions unique to each individual pathogen. Resolution of the mix of amplified products is achieved by PCR product hybridization to corresponding probe sequences,…
![blue bacteria](/sites/default/files/styles/scale_exact_400x400_/public/2022-07/blue%20bacteria.jpg?itok=ddcclBXg)
This LLNL-developed invention is multiplexed and utilizes the Luminex bead-based liquid array, which contains 100 different unique beads. Oligonucleotide probes with sequences complementary to the target sequences are covalently coupled to these unique beads. These capture beads are mixed with viral samples obtained from the patient via cheek swabbing or a throat wash and subjected to PCR in a…
![Cow](/sites/default/files/styles/scale_exact_400x400_/public/2022-07/Cow.jpg?itok=ZMhJc1KF)
LLNL scientists have developed a high-confidence, real-time multiplexed reverse transcriptase PCR (RT-PCR) rule-out assay for foot and mouth disease virus (FMDV). It utilizes RT-PCR to amplify both DNA and RNA viruses in a single assay to detect FMDV as well as rule out other viruses that cause symptoms in livestock indistinguishable from those caused by FMDV, such as Bovine Herpes Virus-1 (…
![biosecurity petri dish](/sites/default/files/styles/scale_exact_400x400_/public/2022-07/biosecurity%20petri%20dish.jpg?itok=nHRadA1E)
LLNL researchers have invented a system for identifying all known and unknown pathogenic or non-pathogenic organisms in a sample. This invention takes a complex sample and generates droplets from it. The droplets consist of sub-nanoliter volume reactors which contain the organism sized particles. A lysis device lyses the organisms and releases the nucleic acids. An amplifier then magnifies the…
![passive flow lateral device](/sites/default/files/styles/scale_exact_400x400_/public/2022-07/passive%20flow%20lateral%20device.jpg?itok=_ChAMmkc)
LLNL researchers have developed a portable device which analyzes one or multiple types of body fluids or gases to test for one or more medical conditions. A bodily fluid (such as blood, perspiration, saliva, breath, or urine) is put into a condenser surface and is then separated into both a primarily gas fluid component and a second one that is primarily liquid. These two samples from the same…
![Corona virus](/sites/default/files/styles/scale_exact_400x400_/public/2022-07/coronavirus.jpg?itok=CAaxyotI)
LLNL researchers have developed a method to quickly and accurately identify the family of a virus infecting a vertebrate via PCR. Universal primer sets consisting of short nucleic acid strands of 7 to 30 base pairs in length were created to amplify target sequences of viral DNA or RNA. These primers can amplify certain identifying sequences of all viral genomes sequenced to date as well as…
![image_of_the_device.png image_of_the_device](/sites/default/files/styles/scale_exact_400x400_/public/2019-08/image_of_the_device.png?itok=RQ0-VBQm)
LLNL scientists have developed a battery-powered device which is low-cost and multi-chambered for the extraction and amplification of nucleic acids from environmental, clinical, and laboratory samples via loop-mediated isothermal amplification (LAMP). This platform identifies pathogenic bacteria and assists in determining the optimal treatment plan. A multi-chamber amplification cartridge in…
![Retina](/sites/default/files/styles/scale_exact_400x400_/public/2022-07/retina.jpg?itok=PMxD0RVZ)
LLNL scientists have developed a method to ensure the accuracy of that tomographic image by applying adaptive optics (AO) to OCT in a single instrument (AO-OCT). AO stabilizes the image being captured by the OCT device by utilizing a Hartmann-Shack wavefront sensor and a deformable mirror, a type of mirror designed to compensate for detected waveform abnormalities (such as ones caused by a…
![Autonomous detection, Bio watch, airborne detection](/sites/default/files/styles/scale_exact_400x400_/public/2022-07/autonomous%20detection.jpg?itok=4hu1aQYK)
LLNL scientists have created a standalone pathogen identifier that can be placed in public settings, such as in stores or on street corners. Not unlike an ATM in physical size, this kiosk will accept biological samples from an individual for multiplexed analysis. The sample collection process will be sufficiently simple such that anyone could begin the diagnostic process after making the…
![freeze_casting_porous_materials](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/freeze_casting_porous_materials.png?itok=2twOT_K3)
The LLNL method is based on freeze‐casting of aerosolized and pressurized metal salt solutions and subsequent thermal processing. This method generates both porous particles with sizes down to one micron and macroscopic monoliths with nanometer scale ligaments/struts. The material's density can be controlled during the freeze‐dried stage. Compared to conventional approaches, this method…
![AgAg2S reference electrode](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/AgAg2S%20reference%20electrode.jpg?itok=kL2OzfHy)
LLNL has developed a reference electrode that is a great improvement on the widely used silver or platinum wire QRE commonly used in electrochemistry in ionic liquids. This new reference electrode, based on a silver-sulfide coated silver wire, exhibits greatly improved stability over a QRE. The stability of our RE approaches that of the Ag/Ag+ RE, but unlike the Ag/Ag+ RE, the RE reported here…
![CNT Carbon Nanotube yarns support spherical](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/CNT%20yarns%20support%20spherical.jpg?itok=ndieUaDs)
LLNL has developed a liquid-free method that increases the overall mechanical resistance of self-supported, carbon nanotube assemblies through nanoscale reinforcement by gas-phase deposition of a thermally cross-linkable polymer. Polymer-reinforcement increases the strength of CNT yarns after crosslinking. For example, a minimal amount (<200 nm) of poly-glycidyl metacrylate (PGMA) deposited…
![Bio-Based Shape Memory Polymer](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/Bio-Based%20Shape%20Memory%20Polymer.png?itok=LD-aph8l)
LLNL researchers have developed a novel method of 3D printing regular microstructured architectures and subsequent complex macrostructures from additively manufactured bio-based composite thermoset shape memory polymer composite materials. This technology for 3D additively manufactured parts utilizes up to a 4 axis control DIW system for fabricating bio based thermally cured epoxy based SMP…
![composite_material](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/composite_material1.jpg?itok=fS_as8eL)
LLNL researchers have developed the hardware and chemistry to allow additive manufacturing of short carbon fibers in a thermoset polymer matrix which have a high degree of structural alignment over conventional cast or pressed short/chopped carbon fiber polymer composites.
The invention is based on the shear dispersal, alignment and concentration of fiber fraction within a resin…
![Retina](/sites/default/files/styles/scale_exact_400x400_/public/2022-07/retina.jpg?itok=PMxD0RVZ)
Using various excitation wavelengths, a hyperspectral microscope takes advantage of autofluorescence and polarized light scattering from cellular components to obtain composite images that highlight their presence. The light collection efficiency is maximized to achieve image acquisition times and rates suitable for in vivo applications.
![Laser Peening](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/Laser%20peening.jpg?itok=l2OKtGme)
LLNL’s system consists of one or more flashlamp-pumped Nd:glass zig-zag amplifiers, a very low threshold stimulated-Brillouin-scattering (SBS) phase conjugator system, and a free-running single frequency Nd:YLF master oscillator.
![intracranial hematoma detector](/sites/default/files/styles/scale_exact_400x400_/public/2022-07/intracranial%20hematoma%20detector.jpg?itok=-jBgXVpX)
The patented intracranial hematoma detection technology uses Micropower Impulse Radar (MIR). MIR uses short, high frequency electromagnetic pulses to obtain information in a non-invasive manner. Unlike ultrasound and other electromagnetic techniques, MIR can operate well through the skull, which is of great importance for intracerebral as well as epidural and subdural hematomas. The MIR…
![nuclear reactor](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/nuclear%20reactor.jpg?itok=RMgGfrZv)
The new LLNL technique works by transiently removing and trapping concrete or rock surface material, so that contaminants are confined in a manner that is easy to isolate and remove. Our studies suggest that 10 m2 of surface could be processed per hour. The technique easily scales to more surface/hr.
![metallic_nanospheres.jpg metallic_nanospheres](/sites/default/files/styles/scale_exact_400x400_/public/2019-08/metallic_nanospheres.jpg?itok=-j4nK6vi)
The nanosphere synthesis process works when a nanostructured substrate is heated above a critical temperature in the presence of a small amount of metal on the nanostructured surface. The metal acts as a particular type of catalyst for nanowire formation. It is periodically segregated within the nanowire in a thermodynamically well-defined process as nanowires grow. The result is…
![plants Lattice](/sites/default/files/styles/scale_exact_400x400_/public/2022-06/plantsLattice2_875x500px.jpg?itok=3ArsXjAU)
Redox ion-exchange polymers ("redox-ionites") and membranes possessing cation- and anion- exchange, amphoteric, complex-forming and oxidation-reduction abilities have been developed on the basis of the biocompatible synthetic and chemically modified natural polymers. In addition, developments have been made towards methods of obtaining of water-soluble and spatially cross-linked ionites of…